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The temperature of the pyrolysis chamber was 280 C, except in case of pyrolysis experiments performed at 250 C, when the chamber temperature was set at 250 C as well

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For each brand, we also measured levels of the TSNAs, NNN ( N -nitrosonornicotine), and NNK (4-(methylnitrosamino)-1-(3-pyridyl)-1-butanone) via HPLC-MS, and the nicotine content via GC-FID