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Failures included: Harmonify: 5.893 EU/mL Aqua Science: 5.398 EU/mL Lambda: 0.765 EU/mL Hospira vial #1: 5.013 EU/mL The Hospira failure was later considered a likely method error after repeat testing passed

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4.12 Proteomics and phosphoproteomics data analysis using Perseus Analysis for treatment versus untreated control of peptides and phosphopeptides was performed using Perseus v2.0.9.0