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Synthesis A is the following: 6.72 g of metal iron powder (Riedel-de Ha n, 99%), 64 ml of deionized water and 33.6 ml of 70% perchloric acid in water (Riedel -de Ha n) are mixed with magnetic stirring and heated at 50 C

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Okubo Y, Suwazono Y, Kobayashi E, Nogawa K

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